Research output: Contribution to journal › Article › peer-review
Research output: Contribution to journal › Article › peer-review
}
TY - JOUR
T1 - Crystal structure, magnetic and transport properties of Fe0.25TaSe2
AU - Nosova, N.
AU - Selezneva, N.
AU - Shishkin, D.
AU - Baranov, N.
N1 - This work was supported by the Ministry of Science and Higher Education of Russia (project FEUZ-2023-0017 and theme «Magnet» No.122021000034-9). NMN acknowledges the Program of the Ural Federal University CEP 3.1.1.1–20.
PY - 2024
Y1 - 2024
N2 - The Fe0.25TaSe2 polycrystalline samples have been synthesized using two routes of solid-state reactions and various heat treatments and cooling conditions. The obtained samples have been studied by x-ray diffraction, magnetization and electrical resistivity measurements. It has been revealed that various methods of preparation and heat treatment do not have a strong effect on the lattice parameters of the main phase in the samples, but they significantly affect the magnetic critical temperature and magnetic hysteresis of the samples. Depending on the sample preparation procedure magnetic ordering temperature of Fe0.25TaSe2 is observed to vary in the range 33–60 K. The coercive field values from 31.7 kOe to 65.3 kOe at T = 2 K are indicative of a very high magnetocrystalline anisotropy in this material. The observed distinctions in the magnetic characteristics of the Fe0.25TaSe2 samples obtained by various methods and after different heat treatments can be ascribed to the difference in the distribution of Fe atoms over the crystal lattice.
AB - The Fe0.25TaSe2 polycrystalline samples have been synthesized using two routes of solid-state reactions and various heat treatments and cooling conditions. The obtained samples have been studied by x-ray diffraction, magnetization and electrical resistivity measurements. It has been revealed that various methods of preparation and heat treatment do not have a strong effect on the lattice parameters of the main phase in the samples, but they significantly affect the magnetic critical temperature and magnetic hysteresis of the samples. Depending on the sample preparation procedure magnetic ordering temperature of Fe0.25TaSe2 is observed to vary in the range 33–60 K. The coercive field values from 31.7 kOe to 65.3 kOe at T = 2 K are indicative of a very high magnetocrystalline anisotropy in this material. The observed distinctions in the magnetic characteristics of the Fe0.25TaSe2 samples obtained by various methods and after different heat treatments can be ascribed to the difference in the distribution of Fe atoms over the crystal lattice.
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U2 - 10.1016/j.physb.2023.415492
DO - 10.1016/j.physb.2023.415492
M3 - Article
VL - 673
JO - Physica B: Condensed Matter
JF - Physica B: Condensed Matter
SN - 0921-4526
M1 - 415492
ER -
ID: 49260961