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A parallel Ugi reaction at students laboratories in the Ural and Moscow. / Mironov, M. A.; Babaev, E. V.
In: Russian Journal of General Chemistry, Vol. 80, No. 12, 01.12.2010, p. 2647-2654.

Research output: Contribution to journal › Article › peer-review

Harvard

Mironov, MA & Babaev, EV 2010, 'A parallel Ugi reaction at students laboratories in the Ural and Moscow', Russian Journal of General Chemistry, vol. 80, no. 12, pp. 2647-2654. https://doi.org/10.1134/S1070363210120303

APA

Mironov, M. A., & Babaev, E. V. (2010). A parallel Ugi reaction at students laboratories in the Ural and Moscow. Russian Journal of General Chemistry, 80(12), 2647-2654. https://doi.org/10.1134/S1070363210120303

Vancouver

Mironov MA, Babaev EV. A parallel Ugi reaction at students laboratories in the Ural and Moscow. Russian Journal of General Chemistry. 2010 Dec 1;80(12):2647-2654. doi: 10.1134/S1070363210120303

Author

Mironov, M. A. ; Babaev, E. V. / A parallel Ugi reaction at students laboratories in the Ural and Moscow. In: Russian Journal of General Chemistry. 2010 ; Vol. 80, No. 12. pp. 2647-2654.

BibTeX

@article{9e293f50807043bda10f812a8058c062,
title = "A parallel Ugi reaction at students laboratories in the Ural and Moscow",
abstract = "A four-component Ugi reaction was adapted for students education. To this end, a series of almost odorless aromatic isonitriles with donor substituents was reacted with a specific carboxylic acid, phthaloyl glycine, to obtain poorly soluble (although nicely crystallized) products. The process was performed and compared in two versions by using (1) a standard centrifuge for parallel separation of precipitates and (2) parallel filtration with SynCore apparatus. It is shown for a broad series of aliphatic ketones and benzyl amines that the yields are satisfactory and the products require no further purification.",
author = "Mironov, {M. A.} and Babaev, {E. V.}",
year = "2010",
month = dec,
day = "1",
doi = "10.1134/S1070363210120303",
language = "English",
volume = "80",
pages = "2647--2654",
journal = "Russian Journal of General Chemistry",
issn = "1070-3632",
publisher = "Maik Nauka-Interperiodica Publishing",
number = "12",

}

RIS

TY - JOUR

T1 - A parallel Ugi reaction at students laboratories in the Ural and Moscow

AU - Mironov, M. A.

AU - Babaev, E. V.

PY - 2010/12/1

Y1 - 2010/12/1

N2 - A four-component Ugi reaction was adapted for students education. To this end, a series of almost odorless aromatic isonitriles with donor substituents was reacted with a specific carboxylic acid, phthaloyl glycine, to obtain poorly soluble (although nicely crystallized) products. The process was performed and compared in two versions by using (1) a standard centrifuge for parallel separation of precipitates and (2) parallel filtration with SynCore apparatus. It is shown for a broad series of aliphatic ketones and benzyl amines that the yields are satisfactory and the products require no further purification.

AB - A four-component Ugi reaction was adapted for students education. To this end, a series of almost odorless aromatic isonitriles with donor substituents was reacted with a specific carboxylic acid, phthaloyl glycine, to obtain poorly soluble (although nicely crystallized) products. The process was performed and compared in two versions by using (1) a standard centrifuge for parallel separation of precipitates and (2) parallel filtration with SynCore apparatus. It is shown for a broad series of aliphatic ketones and benzyl amines that the yields are satisfactory and the products require no further purification.

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U2 - 10.1134/S1070363210120303

DO - 10.1134/S1070363210120303

M3 - Article

VL - 80

SP - 2647

EP - 2654

JO - Russian Journal of General Chemistry

JF - Russian Journal of General Chemistry

SN - 1070-3632

IS - 12

ER -

ID: 37838133